CH3OH in methanol (C6H4Br)SiCl3 and CH3OH (1:3 mol);;

in tetrahydrofuran a) RT, overnight, b) reflux, 1 h;

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tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in N,N-dimethyl-formamide; acetonitrile T=100°C; Hiyama Coupling; 3 h; Inert atmosphereGreen chemistry;