2-氟-2,2-二硝基乙醇合成路线 (共 34 条)
反应条件
potassium carbonate in benzene
参考文献
Adolph,H.G.; Kamlet,M.J.
Journal of Organic Chemistry, 1969 , vol. 34, p. 45 - 50
反应条件
ammonium hydroxide in dichloromethane; water
参考文献
Klapoetke, Thomas M.; Krumm, Burkhard; Rest, Sebastian F.; Reynders, Martin; Scharf, Regina
European Journal of Inorganic Chemistry, 2013 , # 34 p. 5871 - 5878
反应条件
ammonium hydroxide in methanol; water 24 h; Heating;
参考文献
Gafurov,R.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1970 , p. 329 - 332
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1970 , # 2 p. 383 - 387
反应条件
in methanol; water 24 h; Heating;
参考文献
Adolph,H.G.; Kamlet,M.J.
Journal of Organic Chemistry, 1969 , vol. 34, p. 45 - 50
反应条件
sodium sulfate in tetrachloromethane 23 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Chapman, Robert D.; Andreshak, John L.; Herrlinger, Stephen P.; Shackelford, Scott A.; Hildreth, Robert A.; Smith, Jeffrey P.
Journal of Organic Chemistry, 1986 , vol. 51, # 20 p. 3792 - 3798
参考文献
Adolph,H.G.; Kamlet,M.J.
Journal of Organic Chemistry, 1969 , vol. 34, p. 45 - 50
反应条件
pyridine; hydrogenchloride in dichloromethane
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US5194103 A1, 1993 ;
反应条件
trifluoroacetic anhydride
参考文献
Cochoy,R.E.; R McGuire,R.
Journal of Organic Chemistry, 1972 , vol. 37, p. 3041 - 3042
参考文献
Oreshko,G.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1973 , vol. 22, # 5 p. 1142 - 1143
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1973 , vol. 22, # 5 p. 1175 - 1176
反应条件
sulfuric acid in dichloromethane
参考文献
Adolph,H.G.; Kamlet,M.J.
Journal of Organic Chemistry, 1969 , vol. 34, p. 45 - 50