(OC-6-11)-六氟-锑酸铯合成路线 （共 25 条）
反应条件
in sulfur dioxide
1 h at -70°C (pptn.); detd. by IR and Raman spectroscopy;
参考文献
Holfter; Klapoetke; Schulz
European Journal of Solid State and Inorganic Chemistry, 1996 , vol. 33, # 9 p. 855 - 864
反应条件
byproducts: BrF3O; addn. at -196°C, stirred at 20°C for 2.5 h, cooled to -196°C; the noncondensable material distd. off, the voleatile material sept. byfractional distn., the solid nonvolatile product determined by Raman spetr.;
参考文献
Christe, Karl O.; Wilson, William W.; Wilson, Richard D.
Inorganic Chemistry, 1980 , vol. 19, p. 1494 - 1498
反应条件
dry air atmosphere; heating (150-200°C, 2-50 h, autoclave); X-ray anal.;
参考文献
Popov, A. I.; Scharabarin, A. V.; Sukhoverkhov, V. F.; Tchumaevsky, N. A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1989 , vol. 576, p. 242 - 254
反应条件
dry air atmosphere; heating (200-300°C, 2-25 h, autoclave);
参考文献
Popov, A. I.; Scharabarin, A. V.; Sukhoverkhov, V. F.; Tchumaevsky, N. A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1989 , vol. 576, p. 242 - 254
反应条件
addn. of HF to a mixture of CsF and NF4SbF6, stirring for 30 min at 25°C, cooling to -78°C, then to -196°C, addn. of CrF5;
参考文献
Bougon, Roland; Wilson, William W.; Christe, Karl O.
Inorganic Chemistry, 1985 , vol. 24, p. 2286 - 2292
