2-6-二甲基-4-硝基苯胺合成路线 （共 19 条）
反应条件
1: With hydrogenchloride; water T=140°C; 0.5 h; Microwave irradiation; 2: With sodium carbonate in water
参考文献
H. LUNDBECK A/S
Patent: WO2006/29623 A1, 2006 ;
Location in patent: Page/Page column 55 ;
WO 2006/029623 A1
反应条件
sulfuric acid T=50°C; 1 h;
参考文献
Moorthy, Jarugu Narasimha; Saha, Satajit
European Journal of Organic Chemistry, 2009 , # 5 p. 739 - 748
反应条件
ammonia in methanol T=70°C; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 10 p. 2820 - 2827
反应条件
ammonia; water T=180°C;
参考文献
Journal of the American Chemical Society, , vol. 62, p. 2995,3001
反应条件
1: 61 percent / pyridine / 4 h / Heating 2: 74 percent / conc. HNO3 / acetic acid; H2O / 4 h / 140 °C 3: 64 percent / aq. H2SO4 / 16 h / 40 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 7 p. 1062 - 1080
反应条件
sulfuric acid T=50°C; 1 h;
参考文献
Leffek, Kenneth T.; Pruszynski, Przemyslaw
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1454 - 1458
反应条件
1: 74 percent / conc. HNO3 / acetic acid; H2O / 4 h / 140 °C 2: 64 percent / aq. H2SO4 / 16 h / 40 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 7 p. 1062 - 1080
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 11, p. 1350,1354
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 73, p. 809,815
参考文献
Journal of Chemical Research, Miniprint, , # 7 p. 701 - 714
