2,2,4,4,6,6-六甲基-8,8-二苯基环四硅氧烷合成路线 (共 7 条)
反应条件
1: Ph2Si(OH)2 With tris(pentafluorophenyl)-borane in anhydrous xylene T=40°C; Inert atmosphere; 2: HMe2SiOSi(Me2)OSi(Me)2H in anhydrous xylene T=40 - 60°C; 2 h; Inert atmosphere;
参考文献
SIVANCE LLC; Wilson, Michael E.
Patent: US2013/79539 A1, 2013 ;
Location in patent: Paragraph 0021 ;
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide T=-10°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
in perdeuterocyclohexane T=25°C; Laser flash photolysisInert atmosphere;
参考文献
Kostina, Svetlana S.; Leigh, William J.
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4377 - 4388
反应条件
in perdeuterocyclohexane T=25°C; Laser flash photolysisInert atmosphere;
参考文献
Kostina, Svetlana S.; Leigh, William J.
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4377 - 4388
参考文献
Andrianow; Jakuschkina
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 457,458; engl.Ausg.S.425