1,3-二甲基-哌啶-2-酮合成路线 （共 8 条）
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
2 h; Heating;
参考文献
Naito, Takeaki; Tanada, Hiromi; Suzuki, Yumiko; Saito, Haruko; Kiguchi, Toshiko; Ninomiya, Ichiya
Heterocycles, 1993 , vol. 36, # 10 p. 2345 - 2366
反应条件
acetic acid; platinum
Hydrogenation;
参考文献
Leonard; Hauck
Journal of the American Chemical Society, 1957 , vol. 79, p. 5279,5286
反应条件
in chloroform
1.) -78 deg C, 2.) 25 deg C;
参考文献
Hoffman, Robert V.; Salvador, James M.
Tetrahedron Letters, 1989 , vol. 30, # 32 p. 4207 - 4210
反应条件
1: und Behandeln des Reaktionsgemisches mit Kalium-hexacyanoferrat(III) und wss.Kalilauge
2: platinum; acetic acid / Hydrogenation
View Scheme
参考文献
Leonard; Hauck
Journal of the American Chemical Society, 1957 , vol. 79, p. 5279,5286
参考文献
Moehrle, H.; Claas, M.
Pharmazie, 1988 , vol. 43, # 11 p. 749 - 753
反应条件
lithium diisopropyl amide
1) THF, hexane, -78 deg C, 30 min, 2) THF, 1 h; Yield given. Multistep reaction;
参考文献
Nobe, Manabu; Itoh, Akichika; Nishide, Kiyoharu; Abe, Hitoshi; Kawabata, Takeo; et al.
Synthesis, 1992 , # 11 p. 1119 - 1124
反应条件
mercury(II) diacetate
other reagent: Hg(II)-EDTA; Product distribution;
参考文献
Moehrle, H.; Claas, M.
Pharmazie, 1988 , vol. 43, # 11 p. 749 - 753
参考文献
Leonard; Sauers
Journal of the American Chemical Society, 1957 , vol. 79, p. 6210,6213
Full Text Show Details
Leonard; Hauck
Journal of the American Chemical Society, 1957 , vol. 79, p. 5279,5286
