反应条件
in neat (no solvent)
CsIF4O2 and NF4SbF6 were placed in flask, HF was condensed in at -78°C, mixt. was stirred for 1 h at room temp., cooled to -78°C,sepd. by filtrtaion, HF was pumped off over several h form -64 to -30°C, residue was decomposed; volatiles products were passed through trap at -78, -95, -112 and -210°C; elem. anal.;
参考文献
Christe, Karl O.; Wilson, Richard D.; Schack, Carl J.
Inorganic Chemistry, 1981 , vol. 20, p. 2104 - 2114
