1-(羟甲基)-4-甲氧基萘合成路线 （共 8 条）
反应条件
sodium tetrahydroborate in ethanol T=50°C; 1 h;
参考文献
Foster, B.; Gaillard, B.; Mathur, N.; Pincock, A. L.; Pincock, J. A.; Sehmbey, C.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1599 - 1607
反应条件
lithium aluminium tetrahydride in diethyl ether 1.) reflux, 3 h; 2.) room temperature, 14 h;
参考文献
Dixon, Elisabeth A.; Fischer, Alfred; Robinson, Frank P.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2629 - 2641
反应条件
1: 1.) Mg / 2.) ether 2: 50 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h; 2.) room temperature, 14 h View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 2629 - 2641
反应条件
1: 74 percent / bromine, iodine / CHCl3 / 1.25 h / 20 °C 2: 1.) Mg / 2.) ether 3: 50 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h; 2.) room temperature, 14 h View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 2629 - 2641
参考文献
Journal of the American Chemical Society, , vol. 84, p. 859 - 862
参考文献
Corrosion Anticorrosion, , vol. 4, p. 4,21
反应条件
sodium tetrahydroborate
1.) DMF, 2.) DMF; Multistep reaction;
参考文献
DeCosta, Dayal P.; Pincock, James A.
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2180 - 2190
反应条件
1: 88 percent / HCl (gas) / diethyl ether / 1 h
2: diethyl ether / 3 h
3: 82 percent / Irradiation
View Scheme
参考文献
Foster, B.; Gaillard, B.; Mathur, N.; Pincock, A. L.; Pincock, J. A.; Sehmbey, C.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1599 - 1607
