3-乙酰基-3-甲基戊烷二腈合成路线 （共 10 条）
反应条件
N-benzyl-trimethylammonium hydroxide in methanol; tert-butyl alcohol T=10 - 20°C;
参考文献
Gray, George W.; Kelly, Stephen M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 26 - 31
反应条件
in Gegenwart eines basischen Anionen-Austauschers;
参考文献
Industrial and Engineering Chemistry, , vol. 44, p. 1388
US2579580 , ;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3699
参考文献
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, , vol. 264, p. 1186 - 1188
反应条件
potassium hydroxide Sieden;
参考文献
US2437906 , ;
Chem.Abstr., , p. 4196
反应条件
1: 74 percent / sodium hydroxide, water / 10 h / Heating 2: 63 percent / acetic anhydride / 14 h / Heating 3: 71 percent / potassium hydroxide, water / 6 h / 70 °C / Heating View Scheme
参考文献
Kraus,W. et al.
Tetrahedron, 1969 , vol. 25, p. 3681 - 3692
参考文献
Colonge,J.; Vuillemet,R.
Bulletin de la Societe Chimique de France, 1961 , p. 1757 - 1759
反应条件
sodium hydroxide in water
参考文献
Magnetic Resonance in Chemistry, , vol. 24, p. 213 - 220
反应条件
1: H2O / Alkaline hydrolysis
2: acetic anhydride / 1 - 3 Torr
View Scheme
参考文献
Gray, George W.; Kelly, Stephen M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 26 - 31
反应条件
1: 92 percent / NaOH / H2O
3: 93 percent / HCl / methanol
4: 90 percent / NH2-NH2, KOH / bis-(2-hydroxy-ethyl) ether
5: 78 percent / CH3COCl, SnCl4
6: 74 percent / CH2Cl2
View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Iyer, V. Sankar; Kok, Gaik B.
Magnetic Resonance in Chemistry, 1986 , vol. 24, p. 213 - 220
