4-甲氧基苯甲酰异硫氰酸酯合成路线 （共 22 条）
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 70 - 80 °C 2: potassium hydroxide / 4 h / pH 1-2 / |Reflux 3: thionyl chloride / 6 h / |Reflux 4: acetonitrile / 1.5 h / |Reflux View Scheme
参考文献
Journal of Molecular Structure, , vol. 1031, p. 43 - 48
反应条件
1: potassium hydroxide / 4 h / pH 1-2 / |Reflux 2: thionyl chloride / 6 h / |Reflux 3: acetonitrile / 1.5 h / |Reflux View Scheme
参考文献
Journal of Molecular Structure, , vol. 1031, p. 43 - 48
反应条件
in acetone T=45 - 50°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 7 p. 1645 - 1649
参考文献
Journal of the Chemical Society, , p. 1163,1167
Journal of the Chemical Society, , p. 1579,1581
反应条件
in acetone 0.5 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 8 p. 2326 - 2328
反应条件
pyridine 12 h; Ambient temperature;
参考文献
Saczewski, Franciszek
Heterocycles, 1994 , vol. 37, # 2 p. 689 - 692
参考文献
Journal of the Chemical Society, , p. 1163,1167
Journal of the Chemical Society, , p. 1579,1581
反应条件
in acetone 4 h; Heating;
参考文献
Synthetic Communications, , vol. 20, # 5 p. 693 - 701
反应条件
1: benzene / 20 °C
2: pyridine / 8 h / 120 °C
View Scheme
参考文献
Singh, Girija S.; Singh, Tarjeet; Lakhan, Ram
Arkivoc, 2012 , vol. 2013, # 2 p. 213 - 219
反应条件
1: P2S5 / xylene / Heating
2: Hg(OAc)2 / acetic acid / 12 h / Ambient temperature
View Scheme
参考文献
Behringer,H.; Bender,D.
Chemische Berichte, 1967 , vol. 100, # 12 p. 4027 - 4041
