1,4-二硫杂螺[4.11]十六烷合成路线 (共 6 条)
反应条件
potassium permanganate; tetrachlorosilane in acetonitrile T=20°C; 0.166667 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 179, # 2 p. 403 - 409
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Wilson, Stephen R.; Georgiadis, Gregory M.; Khatri, Hiralal N.; Bartmess, John E.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3577 - 3583
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78°C; 4 h;
参考文献
Martel, Arnaud; Chewchanwuttiwong, Sopa; Dujardin, Gilles; Brown, Eric
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1491 - 1494
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78°C; 4 h;
参考文献
Martel, Arnaud; Chewchanwuttiwong, Sopa; Dujardin, Gilles; Brown, Eric
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1491 - 1494
反应条件
Envirocat EPZ10R in dichloromethane
4 h; Heating;
参考文献
Gajare; Shingare; Bandgar
Journal of Chemical Research - Part S, 1998 , # 8 p. 452 - 453
反应条件
n-butyllithium in diethyl ether
T=25°C; 6 h;
参考文献
Wilson, Stephen R.; Georgiadis, Gregory M.; Khatri, Hiralal N.; Bartmess, John E.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3577 - 3583