5,6-二氯-1H-吲哚-2,3-二酮合成路线 （共 10 条）
反应条件
sulfuryl dichloride; iodine; acetic acid T=50°C; 8 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 19 p. 5536 - 5549
反应条件
water in methanol 50 h; Heating;
参考文献
Tetrahedron Letters, , vol. 39, # 42 p. 7679 - 7682
参考文献
Journal of the American Chemical Society, , vol. 78, p. 1251,1254
反应条件
1: Na2SO4; aq. HCl; H2NOH*HCl / 2 h / 80 - 90 °C 2: H2SO4 / 0.25 h / 80 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 4 p. 935 - 946
反应条件
1: pyridine*HBr*Br2 / 2-methyl-propan-2-ol; H2O / 16 h 2: 70 percent / H2O / methanol / 50 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 42 p. 7679 - 7682
反应条件
1: 97 percent / NaH / dimethylsulfoxide / 100 °C 2: 95 percent / Sn, HCl / ethanol / Heating 3: pyridine*HBr*Br2 / 2-methyl-propan-2-ol; H2O / 16 h 4: 70 percent / H2O / methanol / 50 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 42 p. 7679 - 7682
反应条件
1: 95 percent / Sn, HCl / ethanol / Heating 2: pyridine*HBr*Br2 / 2-methyl-propan-2-ol; H2O / 16 h 3: 70 percent / H2O / methanol / 50 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 42 p. 7679 - 7682
反应条件
sulfuric acid Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 11 p. 2085 - 2094
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Journal of Organic Chemistry, , vol. 17, p. 149,153
Journal of the American Chemical Society, , vol. 78, p. 1251,1254
反应条件
1: aqueous NaOH; aqueous H2O2
View Scheme
参考文献
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
