反应条件
in diethyl ether
under N2 a soln. of a mixt. of Ph3GeCl and Ph2GeCl2 was treated with an excess of LiAlH4; after hydrolysis the organic layer was dried over Na2SO4, pumped off, chromd. (silica gel, benzene/hexane);
参考文献
Cerveau, Genevieve; Colomer, Ernesto; Corriu, Robert J.P.; Young, J. Colin
Journal of Organometallic Chemistry, 1981 , vol. 205, # 1 p. 31 - 45