2,6-二甲基-2-羟基苯甲醛合成路线 （共 16 条）
反应条件
1: 2,5-Dimethyl-Phenol With triethylamine; magnesium chloride in acetonitrile 0.25 h; 2: formaldehyd 3 h; Heating;
参考文献
Knight, Paul D.; Clarkson, Guy; Hammond, Max L.; Kimberley, Brian S.; Scott, Peter
Journal of Organometallic Chemistry, 2005 , vol. 690, # 23 p. 5125 - 5144
反应条件
dimethyl selenoxide in benzene 2 h; Heating;
参考文献
Syper; Mlochowski
Synthesis, 1984 , vol. NO. 9, p. 747 - 752
反应条件
AlCl3, aluminium chloride in dichloromethane T=-5 - 0°C; Reimer-Tiemann reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 17 p. 2335 - 2338
反应条件
titanium tetrachloride in dichloromethane from -50 to 0 degC;
参考文献
Nicolaou; Koide, Kazunori; Xu, Jinyou; Izraelewicz, Mark H.
Tetrahedron Letters, 1997 , vol. 38, # 21 p. 3671 - 3674
反应条件
potassium meta-periodate; sulfuric acid in ethanol
参考文献
Synthesis, , p. 624 - 625
反应条件
1: LiAlH4 / diethyl ether 2: aq. KIO4, H2SO4 / ethanol View Scheme
参考文献
Synthesis, , p. 624 - 625
反应条件
boric acid; glycerol T=150 - 165°C; und anschliessendes Erwaermen mit wss.H2SO4;
参考文献
Proceedings of the Iowa Academy of Science, , vol. 52, p. 191,195
反应条件
sodium hydroxide 6 h; Heating;
参考文献
Helvetica Chimica Acta, , vol. 72, p. 811 - 824
反应条件
ethylmagnesium bromide; triethylamine 1.) THF, RT, 20 min, 2.) C6H6, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 24, # 12 p. 1757 - 1760
反应条件
1: hydrochloric acid; sodium nitrite / -8 °C / Kochen der Diazoniumsalz-Loesung mit Schwefelsaeure in Gegenwart von Kupfersulfat 2: aluminium chloride; hydrogen chloride View Scheme
参考文献
Journal of the Chemical Society, , p. 2368
Journal of the Chemical Society, , p. 1110
