1: acetonitrile With lithium diisopropyl amide in tetrahydrofuran T=-78°C; 0.5 h; 2: bromomethyl B(pin) in tetrahydrofuran T=20°C; 18 h; Further stages. Title compound not separated from byproducts.;
参考文献
Man, Hon-Wah; Hiscox, William C.; Matteson, Donald S.
Organic Letters, 1999 , vol. 1, # 3 p. 379 - 381