1,2-双(二苯基膦)乙烷合成路线 （共 132 条）
反应条件
potassium hydroxide 1.) DMSO, 20 deg C, 2.) 50 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 3 p. 198 - 208
反应条件
sodium hydrogencarbonate; HBF4*(CH3)2O 1.) CH2Cl2, from -5 to -25 degC, 12h; 2.) water, 0 degC; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9319 - 9322
反应条件
in dichloromethane N2-atmosphere; refluxing (6 d); detd. by NMR spectroscopy;
参考文献
Organometallics, , vol. 18, # 18 p. 3637 - 3648
反应条件
in chloroform-d1 NMR tube, 40°C (1 d); chromy. (CH2Cl2 / pentane = 3 : 1);
参考文献
Organometallics, , vol. 18, # 18 p. 3637 - 3648
反应条件
2: not given View Scheme
参考文献
Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
in dichloromethane mixing of the Mo compd. with the free phosphine (molar ratio 3.7:1) in CH2Cl2; a molar artio of 2.1:1 yields an equilibrium;;
参考文献
Poli, Rinaldo; Owens, Beth E.; Krueger, Steven T.; Rheingold, Arnold L.
Polyhedron, 1992 , vol. 11, p. 2301 - 2312
反应条件
in tetrahydrofuran N2 atm. (Schlenk techniques used);;
参考文献
Inorganica Chimica Acta, , vol. 205, p. 239 - 244
反应条件
in dichloromethane mixing of the Mo compd. with the free phosphine (molar ratio 2.2:1) in CH2Cl2;; equilibrium;;
参考文献
Polyhedron, , vol. 11, p. 2301 - 2312
反应条件
in N,N-dimethyl-formamide Co(BH3CN)2(Diphos)(DMF) was dissolved in DMF.; Addn. of ether produced crystals of Co(BH3CN)2(DMF)4.;
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 1770 - 1775
反应条件
in chloroform dppe was added to Pt complexin CHCl3 and left to stand at 0°C for20 min;
参考文献
Bokach, Nadezhda A.; Kukushkin, Vadim Yu.; Haukka, Matti; Frausto da Silva, Joao J. R.; Pombeiro, Armando J. L.
Inorganic Chemistry, 2003 , vol. 42, # 11 p. 3602 - 3608
