1,2-双(二苯基膦)乙烷合成路线 （共 132 条）
反应条件
in tetrahydrofuran; ethanol stirring for 2 h; evapn., washing with H2O, drying at 80°C for 12 h;
参考文献
Inorganic Chemistry, , vol. 30, p. 125 - 130
反应条件
in dichloromethane under N2, addn. of complex in CH2Cl2 to soln. of ligand in CH2Cl2, stirred for 25°C for 2 h, white pptn.; evapd. under reduced press., addn. of toluene, heated under reflux for 4 h, yellow pptn., filtered, dried in vac.;
参考文献
Polyhedron, , vol. 12, p. 721 - 730
反应条件
in dimethyl sulfoxide room temp., 30 min; monitored by (1)H NMR;
参考文献
Polyhedron, , vol. 40, # 1 p. 168 - 174
反应条件
1: benzene 2: HCl / chloroform View Scheme
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1698 - 1702
反应条件
in not given (N2); ligand added to a soln. of Pd complex;
参考文献
Dalton Transactions, , # 4 p. 609 - 616
反应条件
in benzene stirring at 298 K for 10 min; pptd. PdCl2(dppe) collected by filtration, bis-aldoximato complex obtained from green filtrate;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1698 - 1702
反应条件
in chloroform-d1 mixing at 240 K, standing; not sepd.; NMR spectroscopy;
参考文献
Polyhedron, , vol. 18, # 20 p. 2583 - 2595
反应条件
in chloroform-d1 40°C, 30 min;
参考文献
Dalton Transactions, , # 12 p. 2210 - 2216
参考文献
Matsui
Yuki Gosei Kagaku Kyokaishi, 1950 , vol. 8, # 9 p. 27,30
Chem.Abstr., 1953 , p. 814
反应条件
in benzene-d6 dissolved in C6D6; crystals were obtained after several weeks in a sealed tube, NMR;
参考文献
Inorganic Chemistry, , vol. 29, p. 3680 - 3685
