1,2-双(二苯基膦)乙烷合成路线 （共 132 条）
反应条件
cesium hydroxide; 4 Angstroem MS in N,N-dimethyl-formamide T=23°C; 36 h;
参考文献
Han, Taek Kyu; Ok, Myung Ahn; Chae, Sung Seok; Kang, Sang Ook; Jung, Jae Ho
Patent: US2010/137669 A1, 2010 ;
Location in patent: Page/Page column 9 ;
反应条件
1,1,3,3-tetramethyldisiloxane; titanium(IV) isopropylate in various solvent(s) T=100°C; 7 h;
参考文献
Berthod, Mikael; Favre-Reguillon, Alain; Mohamad, Jahjah; Mignani, Gerard; Docherty, Gordon; Lemaire, Marc
Synlett, 2007 , # 10 p. 1545 - 1548
反应条件
potassium tert-butylate in dimethyl sulfoxide T=20°C;
参考文献
Tetrahedron Letters, , vol. 43, # 33 p. 5817 - 5819
反应条件
methyl-diethoxy-silane; di-p-nitrophenylphosphoric acid in toluene T=110°C; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yuehui; Lu, Liang-Qiu; Das, Shoubhik; Pisiewicz, Sabine; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2012 , vol. 134, # 44 p. 18325 - 18329
反应条件
lithium in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Bricklebank, Neil; Godfrey, Stephen M.; McAuliffe, Charles A.; Deplano, Paula; Mercuri, Marie L.; Sheffield, Joanne M.
Journal of the Chemical Society - Dalton Transactions, 1998 , # 14 p. 2379 - 2382
反应条件
potassium hydroxide in water; dimethyl sulfoxide 1 h;
参考文献
Khachatryan, R. A.; Sayadyan, S. V.; Grigoryan, N. Yu.; Indzhikyan, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 11 p. 2472 - 2478,2197 - 2203
反应条件
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
参考文献
Folest, J. C.; Nedelec, J. Y.; Perichon, J.
Tetrahedron Letters, 1987 , vol. 28, # 17 p. 1885 - 1886
反应条件
n-butyllithium in tetrahydrofuran -78 deg C, 10 min, RT, 30 min;
参考文献
Chou, Ta-Shue; Tsao, Chung-Huang; Hung, Su Chun
Journal of Organometallic Chemistry, 1986 , vol. 312, p. 53 - 58
反应条件
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s) Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
参考文献
Folest, J. C.; Nedelec, J. Y.; Perichon, J.
Tetrahedron Letters, 1987 , vol. 28, # 17 p. 1885 - 1886
反应条件
sodium und Umsetzung mit 1,2-Dibrom-aethan;
参考文献
Chemische Berichte, , vol. 92, p. 3175,3181
