alpha-叔丁基-alpha-苯基-苯甲醇合成路线 （共 37 条）
反应条件
in tetrahydrofuran
T=-78°C; P=760 Torr; 0.166667 h;
参考文献
Nudelman, N. Sbarbati; Vitale, Arturo A.
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4625 - 4626
反应条件
sodium hydride; zinc(II) chloride in tetrahydrofuran
12 h; Ambient temperature;
参考文献
Uchiyama, Masanobu; Furumoto, Shozo; Saito, Mariko; Kondo, Yoshinori; Sakamoto, Takao
Journal of the American Chemical Society, 1997 , vol. 119, # 47 p. 11425 - 11433
反应条件
in diethyl ether
Ambient temperature;
参考文献
Lomas, John S.; Briand, Sylvette; Fain, Dominique
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 166 - 175
参考文献
Arnold; Bank; Liggett
Journal of the American Chemical Society, 1941 , vol. 63, p. 3444
反应条件
in diethyl ether
1) -5 deg C, 2) 20 deg C;
参考文献
Zarkadis, Antonios K.; Neumann, Wilhelm P.; Marx, Rainer; Uzick, Wolfram
Chemische Berichte, 1985 , vol. 118, # 2 p. 450 - 456
反应条件
in tetrahydrofuran
T=-78°C; P=760 Torr; 0.25 h;
参考文献
Vitale, Arturo A.; Doctorovich, F.; Nudelman, N. Sbarbati
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 9 - 18
反应条件
bis-(pyridin-2-yl)amine; n-butyl-sodium in hexane
T=20°C; 18 h; Inert atmosphereSchlenk techniqueReflux;
参考文献
Armstrong, David R.; Garden, Jennifer A.; Kennedy, Alan R.; Mulvey, Robert E.; Robertson, Stuart D.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7190 - 7193
Angew. Chem., 2013 , vol. 125, # 28 p. 7331 - 7334,4
参考文献
Lorand,J.P.; Wallace,R.W.
Journal of the American Chemical Society, 1974 , vol. 96, # 5 p. 1402 - 1407
反应条件
in hexane
T=20°C; 18 h; Inert atmosphereSchlenk techniqueReflux;
参考文献
Armstrong, David R.; Garden, Jennifer A.; Kennedy, Alan R.; Mulvey, Robert E.; Robertson, Stuart D.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7190 - 7193
Angew. Chem., 2013 , vol. 125, # 28 p. 7331 - 7334,4
参考文献
Schlenk
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 196
