反应条件
1: 2-bromo-2'-methylbiphenyl With n-butyllithium in tetrahydrofuran T=-78°C; Metallation; 1.16667 h; 2: chloro-dicyclohexylphosphine in tetrahydrofuran Condensation; a) -78 deg C, 20 min, b) 0 deg C, 20 min, c) RT, 18 h;
参考文献
Wolfe, John P.; Singer, Robert A.; Yang, Bryant H.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1999 , vol. 121, # 41 p. 9550 - 9561