sodium perchlorate in acetonitrile in electrochemical cell: Pt anode and cathode;
参考文献
Kargin, Yu. M.; Nikitin, E. V.; Parakin, O. V.; Romanov, G. V.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 55 - 58
in methanol; benzene addn. of PPh(OEt)2 to the Re compd. in benzene under inert gas flow and refluxing for 1-2 h, concn. (vac.), addn. of MeOH, heating and concn. at elevated temp.; concn. (vac.), addn. of MeOH, concn. without heating, filtn., washing with Et2O and drying in vac.; elem. anal.;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
in methanol; benzene byproducts: HCl; addn. of PPh(OEt)2 to the Re compd. in benzene under inert gas flow, refluxing for 2 h, concn. (vac.), addn. of MeOH, heating and concn. at elevated temp.; filtn., washing with MeOH-Et2O and drying in vac.; elem. anal.;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
Arshinova,R.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, # 7 p. 1408 - 1412
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, # 7 p. 1518 - 1522
1: 78 percent / ethyl iodide / 48 h / 95 °C
2: oxalyl chloride / 0.67 h / 20 °C
3: triethylamine / diethyl ether / 24 h / 20 °C
View Scheme
参考文献
Nowlan, Charity; Li, Yingchun; Hermann, Johannes C.; Evans, Timothy; Carpenter, Joseph; Ghanem, Eman; Shoichet, Brian K.; Raushel, Frank M.
Journal of the American Chemical Society, 2006 , vol. 128, # 49 p. 15892 - 15902
