P,P-二(3,5-二甲基苯基)-N,N-二乙基亚膦酰胺合成路线 （共 18 条）
反应条件
in hexane T=-78 - 20°C; 12 h;
参考文献
Contreras, Rosalinda; Grevy, Jean Michel; Garcia-Hernandez, Zureima; Goeizado-Rodriguez, Marisol; Wrackmeyer, Bernd
Heteroatom Chemistry, 2001 , vol. 12, # 6 p. 542 - 550
反应条件
in tetrahydrofuran; diethyl ether T=5 - 10°C;
参考文献
RajanBabu; Ayers, Timothy A.; Halliday, Gary A.; You, Kimberly K.; Calabrese, Joseph C.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 6012 - 6025
反应条件
in diethyl ether T=20°C; 3 h;
参考文献
Kato, Shinzi; Goto, Masahisa; Hattori, Rikizoh; Nishiwaki, Koh-ichi; Mizuta, Masateru; Ishida, Masaru
Chemische Berichte, 1985 , vol. 118, # 4 p. 1668 - 1683
参考文献
Abel,E.W. et al.
Journal of the Chemical Society, 1965 , p. 57 - 61
反应条件
in benzene ice cooling;
参考文献
Horner, Leopold; Jordan, Manfred
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 235 - 242
反应条件
1: sulfur / chloroform / 2 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: ammonia; sodium; tetrahydrofuran / 0.08 h / -78 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Stankevic, Marek; Wlodarczyk, Adam; Nieckarz, Damian
European Journal of Organic Chemistry, 2013 , # 20 p. 4351 - 4371
反应条件
1: sulfur / chloroform / 2 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: ammonia; sodium; tetrahydrofuran / 0.08 h / -78 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
European Journal of Organic Chemistry, , # 20 p. 4351 - 4371
反应条件
T=100°C; 1 h; Yield given;
参考文献
Horner, Leopold; Jordan, Manfred
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 235 - 242
参考文献
Ivanov, B. E.; Krokhina, S. S.; Chichkanova, T. V.; Ageeva, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 12 p. 2535 - 2539
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 12 p. 2765 - 2769
参考文献
Petrov,K.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, p. 2377 - 2380,2214 - 2217
