4,4,5,5-四甲基-1,3,2-二氧磷杂环戊烷-2-醇合成路线 （共 23 条）
反应条件
phosphonic acid; dicyclohexyl-carbodiimide in tetrahydrofuran T=20°C; Esterification;
参考文献
Munoz, Aurelio; Hubert, Cathy; Luche, Jean-Louis
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 6015 - 6017
反应条件
water in tetrahydrofuran 2 h;
参考文献
Tromelin, Anne; El Manouni, Driss; Burgada, R.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 301 - 312
反应条件
in toluene T=90°C; 1.5 h;
参考文献
Page, Patrick; Mazieres, Marie-Rose; Bellan, Jacques; Sanchez, Michel
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 70, # 3/4 p. 205 - 210
反应条件
T=130 - 140°C; P=150 Torr; 4 h;
参考文献
Maffei, Michel; Buono, Gerard
Tetrahedron, 2003 , vol. 59, # 44 p. 8821 - 8825
反应条件
benzoic acid in benzene T=70°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 4161 - 4163
反应条件
1H-tetrazole; water in dichloromethane T=20°C; Hydrolysis; 1 h;
参考文献
Heterocycles, , vol. 52, # 2 p. 799 - 810
反应条件
dimethyl amine in benzene T=70°C; 1 h;
参考文献
Bulletin de la Societe Chimique de France, , p. 4161 - 4163
反应条件
1: 75 percent Spectr. / 0.03 h / 140 °C 2: 75 percent Spectr. 3: 48 percent / H2O / CH2Cl2 / 0.17 h / Ambient temperature 4: 15 percent Spectr. / CDCl3 / 96 h / Ambient temperature View Scheme
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 24, p. 235 - 242
反应条件
1: 75 percent Spectr. 2: 48 percent / H2O / CH2Cl2 / 0.17 h / Ambient temperature 3: 15 percent Spectr. / CDCl3 / 96 h / Ambient temperature View Scheme
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 24, p. 235 - 242
反应条件
in butan-1-ol T=105°C;
参考文献
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, , vol. 270, p. 1426 - 1429
