反应条件
potassium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide byproducts: Et2Ge(H)2; Small pieces of K are placed in an ampoule containing HMPA and THF, after stirring for 30 min dissolved Et2Ge(H)2 in THF is gradually added, the react. mixt. is stirred for 24 h, then EtBr is added.; Addn. of water and hexane, organic layer is examined.;
参考文献
Journal of Organometallic Chemistry, , vol. 369, p. 29 - 42
