3,5-二-叔-丁基-4-羟基苯甲酸乙酯合成路线 （共 15 条）
反应条件
sulfuric acid Esterification; 216 h; Heating;
参考文献
Mandal, Subrata; Macikenas, Dainius; Protasiewicz, John D.; Sayre, Lawrence M.
Journal of Organic Chemistry, 2000 , vol. 65, # 16 p. 4804 - 4809
反应条件
potassium hydroxide; ethanol; oxygen T=0 - 5°C; 10 h;
参考文献
Volod'kin, A. A.; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 7 p. 1417 - 1420
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 7 p. 1594 - 1597
反应条件
triethylamine in benzene T=-10 - 0°C; Esterification; 0.5 h;
参考文献
Badea, Florin; Costea, Ion; Velter, Ingrid; Simion, Alina; Simion, Cristian
Revue Roumaine de Chimie, 1999 , vol. 44, # 1 p. 95 - 98
反应条件
hydrogenchloride Erwaermen des Reaktionsprodukts mit NaHCO3 in wss. Aethanol;
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
1: NH2OH*HCl, Py / ethanol; methanol / Heating 2: H2SO4 / Heating 3: aq. NaOH / Heating 4: SOCl2 / Heating View Scheme
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
potassium hydroxide; oxygen T=0 - 5°C; 10 h;
参考文献
Volod'kin, A. A.; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 7 p. 1417 - 1420
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 7 p. 1594 - 1597
反应条件
2: ethanolic HCl / Erwaermen des Reaktionsprodukts mit NaHCO3 in wss. Aethanol View Scheme
参考文献
Cohen
Journal of Organic Chemistry, 1957 , vol. 22, p. 1333
反应条件
1: aq. NaOH / Heating 2: SOCl2 / Heating View Scheme
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
2: aq. NaOH / Heating 3: SOCl2 / Heating View Scheme
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
sulfuric acid Heating;
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
