1: methyl malonic acid diethylester With sodium ethanolate in ethanol T=50°C; Inert atmosphere; 2: methyl iodide in ethanol T=20 - 50°C; Inert atmosphere;
参考文献
Long, Mark; Thornthwaite, David W.; Rogers, Suzanne H.; Bonzi, Gwenaelle; Livens, Francis R.; Rannard, Steve P.
Chemical Communications, 2009 , # 42 p. 6406 - 6408
1: 70 percent / NaH / dimethylformamide; benzene / 2 h / Ambient temperature 2: TBAF / <Cob(II)7C1ester>ClO4 / dimethylformamide / 20 h / 20 °C / electrolysis with Pt electrodes, with warious time, potential, additives, and irradiation View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 1 p. 311 - 324
