3-(1-萘基)-2-丙炔-1-醇合成路线 （共 7 条）
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-butylamine in diethyl ether 5 h;
参考文献
Wu, Ming-Jung; Lin, Chi-Fong; Chang, Li-Juan; Jing, Pao-Tzu; Duh, Tsai-Hui; Tseng, Wuan-Ting; Lee, Fang-Chen; Wang, Shan-Shue; Chang, Hsueh-O.
Journal of the Chinese Chemical Society, 1998 , vol. 45, # 6 p. 783 - 788
反应条件
copper(l) iodide; potassium carbonate; Tedicyp; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=100°C; Sonogashira reaction; 20 h;
参考文献
Feuerstein, Marie; Berthiol, Florian; Doucet, Henri; Santelli, Maurice
Synthesis, 2004 , # 8 p. 1281 - 1289
反应条件
1: 1-ethynylnaphthalene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: formaldehyd in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere;
参考文献
Matouosva, Eliska; Ruzicka, Ales; Kunes, Jiri; Kralova, Jarmila; Pour, Milan
Chemical Communications, 2011 , vol. 47, # 33 p. 9390 - 9392
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 2 h / Reflux 2: CSA / ethanol / Reflux View Scheme
参考文献
Braverman, Samuel; Pechenick-Azizi, Tatiana; Gottlieb, Hugo E.; Sprecher, Milon
Synthesis, 2011 , # 11 p. 1741 - 1750
反应条件
(i) (heating), Py, (ii) aq. H2SO4; Multistep reaction;
参考文献
Atkinson,R.E. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2173 - 2176
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0°C; 0.333333 h;
参考文献
Crich, David; Wu, Baolin
Organic Letters, 2006 , vol. 8, # 21 p. 4879 - 4882
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=20°C; 12 h;
参考文献
Wessig, Pablo; Mueller, Gunnar
Chemical Communications, 2006 , # 43 p. 4524 - 4526
