甲磺酸-2-丙炔-1-醇合成路线 （共 22 条）
反应条件
triethylamine in dichloromethane T=0°C; 2 h;
参考文献
Jackson, W. Roy; Perlmutter, Patrick; Smallridge, Andrew J.
Australian Journal of Chemistry, 1988 , vol. 41, # 8 p. 1201 - 1208
反应条件
sodium azide in 1,4-dioxane T=20°C; 24 h;
参考文献
Loren, Jon C.; Sharpless, K. Barry
Synthesis, 2005 , # 9 art. no. C01005SS, p. 1514 - 1520
反应条件
1: 1-n-heptyne With ethyl magnesium chloride in tetrahydrofuran; diethyl ether 2 h; Heating; 2: methanesulfonic acid prop-2-ynyl ester With copper(l) iodide in tetrahydrofuran; diethyl ether T=0 - 20°C; Further stages.;
参考文献
Kang, Baldip; Britton, Robert
Organic Letters, 2007 , vol. 9, # 24 p. 5083 - 5086
反应条件
trimethyltin radical Multistep reaction;
参考文献
Culshaw, Peter N.; Walton, John C.
Tetrahedron Letters, 1990 , vol. 31, # 17 p. 2457 - 2460
反应条件
tri-n-butylhexadecylphosphonium bromide in toluene T=60°C; 4 h;
参考文献
Jackson, W. Roy; Perlmutter, Patrick; Smallridge, Andrew J.
Australian Journal of Chemistry, 1988 , vol. 41, # 8 p. 1201 - 1208
反应条件
magnesium bromide in diethyl ether T=15°C; 1 h;
参考文献
Place, Pierre; Verniere, Catherine; Gore, Jacques
Tetrahedron, 1981 , vol. 37, p. 1359 - 1368
反应条件
caesium carbonate; potassium iodide in acetonitrile T=70°C;
参考文献
Rivara, Mirko; Patel, Manoj K.; Amori, Laura; Zuliani, Valentina
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 20 p. 6401 - 6404
参考文献
Jackson, W. Roy; Perlmutter, Patrick; Smallridge, Andrew
Tetrahedron Letters, 1988 , vol. 29, # 16 p. 1983 - 1984
反应条件
In(ONf)3 in anhydrous butyl ether 24 h; Inert atmosphere;
参考文献
Tsuchimoto, Teruhisa; Matsubayashi, Hiromichi; Kaneko, Masayoshi; Nagase, Yuta; Miyamura, Takuhiro; Shirakawa, Eiji
Journal of the American Chemical Society, 2008 , vol. 130, # 47 p. 15823 - 15835
反应条件
in acetonitrile T=20°C; 20 h; Inert atmosphere;
参考文献
Zhang, Xiaoxia; Yao, Tuanli; Campo, Marino A.; Larock, Richard C.
Tetrahedron, 2010 , vol. 66, # 6 p. 1177 - 1187
