1-丙基-1H-咪唑-2-甲醛合成路线 （共 6 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Seto, Masaki; Miyamoto, Naoki; Aikawa, Katsuji; Aramaki, Yoshio; Kanzaki, Naoyuki; Iizawa, Yuji; Baba, Masanori; Shiraishi, Mitsuru
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 363 - 386
反应条件
potassium carbonate in N,N-dimethyl-formamide T=50°C;
参考文献
Journal of Biological Chemistry, , vol. 286, # 22 p. 19422 - 19430
反应条件
potassium carbonate in N,N-dimethyl-formamide T=50°C;
参考文献
WO2011/130661 A1, ;
Page/Page column 134 ;
反应条件
1: 1H-imidazole With potassium hydroxide in acetone 2 h; 2: propyl bromide in acetone
参考文献
Kleyi, Phumelele; Walmsley, Ryan S.; Gundhla, Isaac Z.; Walmsley, Tara A.; Jauka, Tembisa I.; Dames, Joanna; Walker, Roderick B.; Torto, Nelson; Tshentu, Zenixole R.
South African Journal of Chemistry, 2012 , vol. 65, p. 231 - 238
反应条件
lithium aluminium tetrahydride in tetrahydrofuran cooling;
参考文献
Seto, Masaki; Miyamoto, Naoki; Aikawa, Katsuji; Aramaki, Yoshio; Kanzaki, Naoyuki; Iizawa, Yuji; Baba, Masanori; Shiraishi, Mitsuru
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 363 - 386
反应条件
1: With methyllithium in tetrahydrofuran; diethyl ether
T=-78 - 20°C; 1 h;
2: With hydrogenchloride in tetrahydrofuran; diethyl ether; water
T=0°C;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1422228 A1, 2004 ;
Location in patent: Page 236 ;
EP 1422228 A1
