1,1,1,3,5,7,7,7-八甲基四硅氧烷合成路线 （共 9 条）
反应条件
water in hexane; water addn. of (CH3)HSiCl2 to ice, (CH3)3SiOSi(CH3)3 and hexane; stirring of the mixt. with concd. H2SO4 at room temp. for 2 h;;
参考文献
US2595890 , ;
C. A., , p. 7820
GB632954 , ;
C. A., , p. 7866
反应条件
trimethylsilyl trifluoromethanesulfonate 24 h;
参考文献
US2007/249502 A1, ;
Page/Page column 18 ;
反应条件
sulfuric acid in water 0.5 h;
参考文献
Scheim, U.; Ruehlmann, K.; Grosse-Ruyken, H.; Porzel, A.
Journal of Organometallic Chemistry, 1986 , vol. 314, p. 39 - 46
反应条件
water in toluene T=20°C; 27 h; Further byproducts given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
water in toluene T=20°C; 27 h; Further byproducts given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
参考文献
Bulletin of the Chemical Society of Japan, , vol. 29, p. 547
反应条件
water in toluene T=20°C; 27 h; hydrolytic copolycondensation depending on final concentration of hydrochloric acid; other dialkyldichlorosilanes; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
Behandeln des Reaktionsprodukts mit konz.H2SO4; Produkt 5: Tris-trimethylsiloxy-methyl-silan;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 963
反应条件
1: 65 percent / Jonol / CCl4 2: 83 percent / NaHCO3 / H2O; diethyl ether / 1 h View Scheme
参考文献
Scheim, U.; Ruehlmann, K.; Grosse-Ruyken, H.; Porzel, A.
Journal of Organometallic Chemistry, 1986 , vol. 314, p. 39 - 46
