1-苯基-2-环己基乙烷合成路线 (共 30 条)
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate T=20°C; 8 h;
参考文献
BAYER SCHERING PHARMA AKTIENGESELLSCHAFT; GRAHAM, Keith; BERNDT, Mathias; CHI, Dae, Yoon; LEE, Byoung, Se; SHINDE, Sandip, S.; KIL, Hee, Seup; LEE, Sang, Ju; RYU, Jin-Sook; OH, Seung, Jun
Patent: WO2011/6610 A1, 2011 ;
Location in patent: Page/Page column 27 ;
反应条件
P(t-Bu)2Me*HBF4; tetrabutyl ammonium fluoride; palladium (II) bromide in tetrahydrofuran T=20°C; Hiyama coupling; 14 h;
参考文献
Lee, Jae-Young; Fu, Gregory C.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5616 - 5617
反应条件
MmNi3.5Co0.7Al0.8H4 T=160°C; P=3677.5 Torr; 3 h;
参考文献
Nakagawa, Shin-ichi; Murata, Satoru; Sakai, Tetsuo; Nomura, Masakatsu
Chemistry Letters, 1994 , # 3 p. 431 - 432
反应条件
sodium tetrahydroborate; tributyltin chloride in ethanol T=25°C; Irradiation;
参考文献
Giese, Bernd; Gonzales-Gomez, Juan Antonio; Witzel, Tom
Angewandte Chemie, 1984 , vol. 96, # 1 p. 51 - 52
反应条件
sodium tetrahydroborate in dichloromethane T=0 - 5°C; 0.5 h;
参考文献
Giese, Bernd; Kretzschmar, Gerhard
Chemische Berichte, 1983 , vol. 116, # 9 p. 3267 - 3270
反应条件
benzil in cyclohexane Irradiation;
参考文献
Li, Yu-Zhuo; Schuster, Gary B.
Journal of Organic Chemistry, 1986 , vol. 51, # 20 p. 3804 - 3811
反应条件
Raney Ni-Al alloy; water; potassium hydroxide T=90°C; 7 h;
参考文献
Liu, Guo-Bin; Zhao, Hong-Yun; Dai, Lu; Thiemann, Thies; Tashiro, Hideki; Tashiro, Masashi
Journal of Chemical Research, 2009 , # 9 p. 579 - 581
反应条件
hydrogen; copper(l) chloride; zinc(II) chloride T=400°C;
参考文献
Nakatsuyi,Y. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 618 - 624
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Schiess,P.; Suter,C.
Helvetica Chimica Acta, 1971 , vol. 54, p. 2636 - 2645
反应条件
dicarbonyl(η5-cyclopentadienyl)iron dimer (I) in benzene T=15 - 20°C; Irradiationother condition: other solvent; Yield given. Yields of byproduct given;
参考文献
Giese, Bernd; Thoma, Gebhard
Helvetica Chimica Acta, 1991 , vol. 74, # 5 p. 1135 - 1142