1-仲-丁基-2-甲基苯合成路线 (共 25 条)
反应条件
C39H61FeN2O4 in diethyl ether T=100°C; Kumada coupling reaction; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Hasan, Kamrul; Dawe, Louise N.; Kozak, Christopher M.
European Journal of Inorganic Chemistry, 2011 , # 29 p. 4610 - 4621
反应条件
iron(III) chloride amine-bis(phenolate) complex in diethyl ether; dichloromethane 0.5 h;
参考文献
Chowdhury, Rajoshree Roy; Crane, Angela K.; Fowler, Candace; Kwong, Philip; Kozak, Christopher M.
Chemical Communications, 2008 , # 1 p. 94 - 96
反应条件
butyl cations; oxygen T=24°C; P=750 Torr; other pressure, concurrent reaction with toluene; Product distribution;
参考文献
Cacace, Fulvio; Ciranni, Giovanna; Giacomello, Pierluigi
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1513 - 1516
反应条件
C54H80Cl2Fe2N2O4 in diethyl ether T=100°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Qian, Xin; Dawe, Louise N.; Kozak, Christopher M.
Dalton Transactions, 2011 , vol. 40, # 4 p. 933 - 943
反应条件
indium trifluoromethanesulfonate; 1-ethyl-3-methylimidazolium bistrifluoromethylsulfonylamide T=120°C; Friedel-Crafts Alkylation; 1.5 h; Microwave irradiationGreen chemistry; Overall yield = 52 percent;
参考文献
Mack, Ryan; Askins, Grant; Lowry, Jacob; Hurley, Nathan; Reeves, Perry C.
Canadian Journal of Chemistry, 2013 , vol. 91, # 12 p. 1262 - 1265
反应条件
1: With zirconocene dichloride T=22 - 23°C; Metallation; cycloalumination; 12 h; 2: With hydrogenchloride Hydrolysis;
参考文献
Ibragimov; Khafizova; Satenov; Khalilov; Yakovleva; Rusakov; Dzhemilev
Russian Chemical Bulletin, 1999 , vol. 48, # 8 p. 1574 - 1580
反应条件
water T=30°C; P=704 Torr; Irradiationeffect of the presence of water, appparent rel. reaction rates; Product distributionMechanism;
参考文献
Cacace, Fulvio; Ciranni, Giovanna; Giacomello, Pierluigi
Journal of the American Chemical Society, 1982 , vol. 104, # 8 p. 2258 - 2261
反应条件
perfluoro-octylsulphonic acid T=100 - 110°C; 14 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fu; He; Lei; Luo
Synthetic Communications, 1991 , vol. 21, # 10-11 p. 1273 - 1279
反应条件
in various solvent(s) T=-22°C; 16 h; Further byproducts given;
参考文献
Russey, William, E.; Haenel, Matthias, W.
Tetrahedron Letters, 1981 , vol. 22, # 41 p. 4065 - 4068
反应条件
in toluene 24 h; Heating; Yield given. Yields of byproduct given;
参考文献
Nitta, Yoshihiro; Arakawa, Yasushi; Ueyama, Naoto
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2710 - 2718