in hexane
byproducts: Me3SiCl; under N2 or Ar; BCl3 condensed in dry-ice cooled dropping funnel; diluted with hexane; dropped (-60°C) into stirred soln. of N(SiMe3)3 inhexane; warmed to room temp.; heated to reflux for 4 h; volatiles removed (25°C, 12 Torr); remaining oil distd. (82°C, 11 Torr);
参考文献
Anand, Benadir; Noeth, Heinrich; Schwenk-Kircher, Holger; Troll, Alexander
European Journal of Inorganic Chemistry, 2008 , # 20 p. 3186 - 3199