反应条件
1: 26.6 g / 18-crown-6 / bis-(2-methoxy-ethyl) ether; tetrahydrothiophene 1,1-dioxide / 15 h / 170 °C 2: 49 percent / LAH / tetrahydrofuran / 20 h / -5 - 0 °C 3: 40 percent / PCC, Na2SO4 / CH2Cl2 / 15 h / Ambient temperature 4: Na2SO4 / benzene / 12 h / Ambient temperature 5: 15 percent Chromat. / benzene / 12 h / 200 °C / other temperature, time, Ea; thermal isomerisation of N-arylmethyl and N-alkyl-2,2-dihalogenocyclopropyl imines, effect of various additivities View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 6 p. 739 - 752
