2-乙酰氧基-2-甲基丙酸合成路线 （共 21 条）
反应条件
in water T=200°C; P=37503.8 Torr; 0.00275 h;
参考文献
Sato, Masahiro; Matsushima, Keiichiro; Kawanami, Hajime; Ikuhsima, Yutaka
Angewandte Chemie - International Edition, 2007 , vol. 46, # 33 p. 6284 - 6288
反应条件
1.) 0 deg C, 50 min; 2.) RT, 20 min; 3.) reflux, 2 h;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1443041 A1, 2004 ;
Location in patent: Page 31 ;
参考文献
Athanasellis, Giorgos; Detsi, Anastasia; Prousis, Kyriakos; Igglessi-Markopoulou, Olga; Markopoulos, John
Synthesis, 2003 , # 13 p. 2015 - 2022
参考文献
Crombie,L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 2976 - 2981
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Anschuetz; Motschmann
Justus Liebigs Annalen der Chemie, 1912 , vol. 392, p. 124
Full Text Show Details
Filachione; Lengel; Fisher
Journal of the American Chemical Society, 1946 , vol. 68, p. 332
反应条件
sulfuric acid; toluene T=110 - 114°C;
参考文献
Fein; Fisher
Industrial and Engineering Chemistry, 1948 , vol. 40, p. 536
反应条件
1: thionyl chloride / 2 h / Heating 2: 52 percent / LiBr / ethyl acetate / 2 h / 80 °C View Scheme
参考文献
Schirmeister-Tichy, Helga; Iacono, Kathryn T.; Muto, Nicholas F.; Homan, Joseph W.; Suhadolnik, Robert J.; Pfleiderer, Wolfgang
Helvetica Chimica Acta, 1999 , vol. 82, # 4 p. 597 - 613
参考文献
Schirmeister-Tichy, Helga; Iacono, Kathryn T.; Muto, Nicholas F.; Homan, Joseph W.; Suhadolnik, Robert J.; Pfleiderer, Wolfgang
Helvetica Chimica Acta, 1999 , vol. 82, # 4 p. 597 - 613
反应条件
triethylamine in acetonitrile Ambient temperatureelectrolysis; Further byproducts given;
参考文献
Thomas, Hans G.; Gabriel, Juergen; Fleischhauer, Joerg; Raabe, Gerhard
Chemische Berichte, 1983 , vol. 116, # 1 p. 375 - 388
反应条件
in acetonitrile Ambient temperatureelectrolysis; Further byproducts given;
参考文献
Thomas, Hans G.; Gabriel, Juergen; Fleischhauer, Joerg; Raabe, Gerhard
Chemische Berichte, 1983 , vol. 116, # 1 p. 375 - 388
反应条件
in acetonitrile Ambient temperatureelectrolysis; MechanismProduct distribution;
参考文献
Thomas, Hans G.; Gabriel, Juergen; Fleischhauer, Joerg; Raabe, Gerhard
Chemische Berichte, 1983 , vol. 116, # 1 p. 375 - 388
