二(4-叔丁基苯基)甲酮合成路线 (共 26 条)
反应条件
AlCl3, aluminium chloride in dichloromethane; water T=0 - 20°C; 29 h;
参考文献
Mitsui Chemicals, Inc.
Patent: EP1548018 A1, 2005 ;
Location in patent: Page/Page column 40 ;
反应条件
aluminium trichloride in various solvent(s) T=25 - 60°C; Acylation; 22 h;
参考文献
Journal of Physical Chemistry A, , vol. 104, # 21 p. 5131 - 5140
反应条件
1,4-diaza-bicyclo[2.2.2]octane in dimethyl sulfoxide T=35 - 40°C; 35 h; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 119, # 38 p. 8795 - 8801
反应条件
1: AlCl3 / CS2 / 36 h / Ambient temperature 2: water / 12 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, # 24 p. 7727 - 7738
反应条件
perchloric acid in tetrachloromethane
参考文献
Volz, Heinrich; Mayer, Wilhelm Dietrich
Liebigs Annalen der Chemie, 1981 , # 8 p. 1424 - 1428
参考文献
Journal of the American Chemical Society, , vol. 68, p. 913
反应条件
water 12 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 108, # 24 p. 7727 - 7738
反应条件
zinc; palladium diacetate in acetone 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1201 - 1202
反应条件
tributyl-amine; oxygen in various solvent(s) 6.5 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 769 - 778
反应条件
1: 85 percent / diethyl ether; cyclohexane / 1) -78 deg C, 30 min, 2) RT, 6h 2: 2) SOCl2 / 1) THF, pentane, -78 deg C, 30 min, 2a) -78 deg C, 30 min, 2b) RT View Scheme
参考文献
Synthesis, , # 12 p. 1179 - 1182