2-甲基-3-喹啉酸乙酯合成路线 (共 33 条)
反应条件
1: With triethylamine; L-proline in dichloromethane T=20°C; 2 h; Inert atmosphere; 2: With triphenylphosphine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Yu, Zhi-Hua; Zheng, Hu-Fei; Yuan, Wei; Tang, Zi-Long; Zhang, Ai-Dong; Shi, De-Qing
Tetrahedron, 2013 , vol. 69, # 38 p. 8137 - 8141
反应条件
tin(ll) chloride; zinc(II) chloride in ethanol T=70°C; 3 h; Molecular sieveInert atmosphere;
参考文献
Nagarapu, Lingaiah; Gaikwad, Hanmant K.; Bantu, Rajashaker
Synlett, 2012 , vol. 23, # 12 p. 1775 - 1778
反应条件
manganese(IV) oxide in ethanol Reflux;
参考文献
Rachakonda, Venkatesham; Alla, Manjula; Kotipalli, Sudha Sravanti; Ummani, Ramesh
European Journal of Medicinal Chemistry, 2013 , vol. 70, p. 536 - 547
反应条件
water T=70°C; Friedlaender reaction; 3 h;
参考文献
Shen, Qiang; Wang, Limin; Yu, Jianjun; Liu, Mingtao; Qiu, Jun; Fang, Lei; Guo, Fenglou; Tang, Jun
Synthesis, 2012 , vol. 44, # 3 art. no. H96411SS, p. 389 - 392
反应条件
anhydrous iron chloride; oxygen; zinc(II) chloride in chlorobenzene T=90°C; 12 h; Molecular sieve;
参考文献
Fan, Jinmin; Wan, Changfeng; Sun, Gaojun; Wang, Zhiyong
Journal of Organic Chemistry, 2008 , vol. 73, # 21 p. 8608 - 8611
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; palladium 10 on activated carbon; acetic acid T=120°C; 15 h; Inert atmosphere; chemoselective reaction;
参考文献
Xing, Rui-Guang; Li, Ya-Nan; Liu, Qiang; Han, Yi-Feng; Wei, Xia; Li, Jing; Zhou, Bo
Synthesis, 2011 , # 13 p. 2066 - 2072
反应条件
ammonium cerium (IV) nitrate in ethanol Friedlaender-Borsche reaction; 3 h; Reflux;
参考文献
Sridharan, Vellaisamy; Ribelles, Pascual; Ramos, Ma. Teresa; Menendez, J. Carlos
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5715 - 5718
反应条件
in N-methyl-acetamide; dichloromethane; water; ethyl acetate; trichlorophosphate
反应条件
hydrogenchloride in water 1 h; Heating;
参考文献
Tetrahedron Letters, , vol. 22, # 30 p. 2893 - 2894
反应条件
hydrogenchloride in water 1 h; Heating;
参考文献
Tetrahedron Letters, , vol. 22, # 30 p. 2893 - 2894