1,4-二乙酰氧基-2-丁烯合成路线 （共 39 条）
反应条件
1,4-bis[4-Oipr-5-(4,5-dihydroIMES)Cl2Ru=CH]pyrimidin-2-ylpiperazine in dichloromethane
T=25°C; 2 h; Inert atmosphere; Reagent/catalyst;
参考文献
Wu, Guang-Long; Cao, Sheng-Li; Chen, Jian; Chen, Zili
European Journal of Organic Chemistry, 2012 , # 34 p. 6777 - 6784
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3 in toluene
T=75 - 85°C; P=52476.2 - 62819.5 Torr; Product distribution / selectivity;
参考文献
Chaudhari, Raghunath Vitthal; Chansarkar, Rashmi; Mukhopadhyay, Kausik; Kelkar, Ashutosh Anant
Patent: US2005/215814 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
toluene-4-sulfonic acid; rhodium on charcoal in benzene
参考文献
Hoffmann-La Roche Inc.
Patent: US4124619 A1, 1978 ;
反应条件
hydrogen; HRh(CO)(PPh3)3-tethered on alumina in toluene
T=70°C; P=52476.2 Torr; Product distribution / selectivity;
参考文献
Chaudhari, Raghunath Vitthal; Chansarkar, Rashmi; Mukhopadhyay, Kausik; Kelkar, Ashutosh Anant
Patent: US2005/215814 A1, 2005 ;
Location in patent: Page/Page column 5 ;
参考文献
Hoffmann-La Roche Inc.
Patent: US4124619 A1, 1978 ;
反应条件
ozone; triphenylphosphine
Yield given. Multistep reaction;
参考文献
Nagasawa, Jun-ichi; Araki, Younosuke; Ishido, Yoshiharu
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1734 - 1736
反应条件
hydrogen; HRh(CO)(PPh3)3-tethered on alumina in toluene
T=70°C; P=52476.2 Torr; Product distribution / selectivity;
参考文献
Chaudhari, Raghunath Vitthal; Chansarkar, Rashmi; Mukhopadhyay, Kausik; Kelkar, Ashutosh Anant
Patent: US2005/215814 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
lithium bromide; tetracarbonylnickel(0)
参考文献
Mettalia,J.B.; Specht,E.H.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3941 - 3947
反应条件
bromine
durch Addition;
参考文献
Griner
Bulletin de la Societe Chimique de France, 1893 , vol. <3>9, p. 218;
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1893 , vol. 117, p. 553
