1-甲氧基-10H-吩噻嗪合成路线 （共 7 条）
反应条件
sodium hydroxide in water T=20°C; Methylation;
参考文献
Yamamura, Tatsuo; Suzuki, Kyouichi; Yamaguchi, Tatsuya; Nishiyama, Tomihiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 413 - 419
反应条件
iodine; sulfur T=175°C;
参考文献
Cadogan,J.I.G.; Kulik,S.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 2621 - 2632
反应条件
1: 46 percent / sulfur; iodine / 2.5 h / 120 - 130 °C 2: 65 percent / NaOH / H2O / 20 °C View Scheme
参考文献
Yamamura, Tatsuo; Suzuki, Kyouichi; Yamaguchi, Tatsuya; Nishiyama, Tomihiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 413 - 419
反应条件
1.1: potassium carbonate; copper / nitrobenzene / 10 h / 200 - 210 °C 1.2: 70 percent / HCl / ethanol / 20 h / Heating 2.1: 55 percent / HBr / acetic acid / 170 h / Heating 3.1: 46 percent / sulfur; iodine / 2.5 h / 120 - 130 °C 4.1: 65 percent / NaOH / H2O / 20 °C View Scheme
参考文献
Yamamura, Tatsuo; Suzuki, Kyouichi; Yamaguchi, Tatsuya; Nishiyama, Tomihiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 413 - 419
反应条件
1.1: potassium carbonate; copper / nitrobenzene / 10 h / 200 - 210 °C 1.2: 70 percent / HCl / ethanol / 20 h / Heating 2.1: 55 percent / HBr / acetic acid / 170 h / Heating 3.1: 46 percent / sulfur; iodine / 2.5 h / 120 - 130 °C 4.1: 65 percent / NaOH / H2O / 20 °C View Scheme
参考文献
Yamamura, Tatsuo; Suzuki, Kyouichi; Yamaguchi, Tatsuya; Nishiyama, Tomihiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 413 - 419
反应条件
3,3,4,4-tetramethyl-1,2-dioxetane in acetonitrile T=15°C; 38 h; Yield given. Yields of byproduct given;
参考文献
Adam, Waldemar; Hueckmann, Sabine; Vargas, Franklin
Tetrahedron Letters, 1989 , vol. 30, # 46 p. 6315 - 6318
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1749 - 1757
