1-溴-2,3,5,6-四氟苯合成路线 （共 15 条）
反应条件
water; phosphorous acid trisdiethylamide in N,N-dimethyl-formamide T=20°C; protodebromination; 0.666667 h;
参考文献
Russian Chemical Bulletin, , vol. 46, # 4 p. 786 - 788
反应条件
bromine T=500 - 510°C;
参考文献
Platonov; Maksimov; Dvornikova; Nikul'shin
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 11 p. 1647 - 1653
反应条件
1: N2H4*H2O / dioxane / Heating 2: aq. CuSO4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 31, p. 746 - 749
参考文献
Journal of Organic Chemistry, , vol. 31, p. 746 - 749
反应条件
in acetonitrile T=150°C; 0.5 h; Microwave irradiationInert atmosphere;
参考文献
Journal of Fluorine Chemistry, , vol. 131, # 5 p. 627 - 634
反应条件
in diethyl ether -20°C, 12 d;
参考文献
Journal of Fluorine Chemistry, , vol. 13, p. 337,339, 340, 344, 348
反应条件
1: diethyl ether 2: diethyl ether View Scheme
参考文献
F: PerFHalOrg.SVol.1, 2.2, page 20 - 27
反应条件
(i) nBuLi, (ii) Br2; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 889 - 892
反应条件
phosphorous acid trisdiethylamide in hexane Dehalogenation; silyldebromination; silyldeprotonation; 3 h;
参考文献
Bardin
Russian Chemical Bulletin, 1997 , vol. 46, # 4 p. 780 - 785
反应条件
trifluorormethanesulfonic acid; SbF5; sodium iodide; Tl(OCOCF3)3 2.) 80 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Deacon, Glen B.; Smith, Richard N.M.
Australian Journal of Chemistry, 1982 , vol. 35, # 8 p. 1587 - 1597
