4,4'-二甲基-2,2'-联(苯酚)合成路线 （共 47 条）
反应条件
boron tribromide in dichloromethane
T=-70 - 20°C;
参考文献
Haberhauer, Gebhard; Tepper, Christina; Woelper, Christoph; Blaeser, Dieter
European Journal of Organic Chemistry, 2013 , # 12 p. 2325 - 2333
反应条件
oxygen; [Co(O2CCH3)2]*4H2O; sodium hydroxide in ethylene glycol
T=80°C; P=760.051 Torr; 9 h;
参考文献
Jiang, Jian-An; Chen, Cheng; Guo, Ying; Liao, Dao-Hua; Pan, Xian-Dao; Ji, Ya-Fei
Green Chemistry, 2014 , vol. 16, # 5 p. 2807 - 2814
反应条件
caesium carbonate; (η5-ethyltetramethylcyclopentadienyl)(η6-benzene)rhodium(III) hexafluorophosphate in water
T=90°C; 24 h;
参考文献
Barrett, Anthony G. M.; Itoh, Toshiyuki; Wallace, Eli M.
Tetrahedron Letters, 1993 , vol. 34, # 14 p. 2233 - 2234
反应条件
aluminium trichloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone in nitromethane
T=25°C; 1 h;
参考文献
Sartori, Giovanni; Maggi, Raimondo; Bigi, Franca; Grandi, Michele
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7271 - 7273
反应条件
diethyl ether; magnesium
anschliessendes Behandeln mit CuCl, Versetzen mit Eis und wss. HCl und Kochen des Reaktionsprodukts mit Essigsaeure und wss. HI;
参考文献
Westerfeld; Lowe
Journal of Biological Chemistry, 1942 , vol. 145, p. 463,466
反应条件
laccase MtL in ethyl acetate
T=30°C; pH=7.5; 24 h; aq. bufferEnzymatic reaction;
参考文献
Navarra, Cristina; Goodwin, Candice; Burton, Stephanie; Danieli, Bruno; Riva, Sergio
Journal of Molecular Catalysis B: Enzymatic, 2010 , vol. 65, # 1-4 p. 52 - 57
反应条件
ammonium cerium(IV) nitrate; dihydrogen peroxide in water
1 h; Ambient temperature;
参考文献
Chakrabarty, Kakoli; Chawla, H. Mohindra; Suresh, Valiya Veettil
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 2 p. 266 - 274
反应条件
1: copper-powder / 275 °C
2: aqueous HI / 170 °C
View Scheme
参考文献
Sugii; Shindo
Yakugaku Zasshi, 1933 , vol. 53, p. 571,576; dtsch. Ref. S. 97
Chem.Abstr., 1934 , p. 151
反应条件
iron(III) chloride in water
T=25°C; 168 h;
参考文献
Asakura, Kouichi; Honda, Eitoshi; Osanai, Shuichi
Chemistry Letters, 1995 , # 7 p. 583 - 584
反应条件
trifluoroacetic acid
T=20°C; 1 h;
参考文献
Endo, Yasuyuki; Shudo, Koichi; Okamoto, Toshihiko
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3769 - 3770
