2-(苯甲酰基)-4,5-二氯哒嗪-3-酮合成路线 (共 20 条)
反应条件
triethylamine in dichloromethane T=-10°C; 0.166667 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
Amberlite(R) IRA-67 in acetonitrile T=20°C; 0.833333 h;
参考文献
Kim, Jeum-Jong; Park, Young-Dae; Kim, Ho-Kyun; Cho, Su-Dong; Kim, Ju-Kyeong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthetic Communications, 2005 , vol. 35, # 5 p. 731 - 738
反应条件
in tetrahydrofuran T=150°C; P=10336 Torr; 0.0833333 h; Microwave irradiation;
参考文献
Kim, Bo Ram; Sung, Gi Hyeon; Ryu, Ki Eun; Kim, Jeum-Jong; Yoon, Yong-Jin
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 11 p. 3410 - 3414
反应条件
1.1: NH2NH2*H2O / tetrahydrofuran / 0.17 h / 20 °C 1.2: tetrahydrofuran / 0.17 h / 20 °C 2.1: polyphosphoric acid / 2 h / 130 °C View Scheme
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Chung, Hyun-A; Kweon, Deok-Heon; Cho, Su-Dong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthesis, 2003 , # 4 p. 560 - 564
反应条件
in tetrahydrofuran T=150°C; P=10336 Torr; 0.0833333 h; Microwave irradiation;
参考文献
Kim, Bo Ram; Sung, Gi Hyeon; Lee, Sang-Gyeong; Yoon, Yong Jin
Tetrahedron, 2013 , vol. 69, # 15 p. 3234 - 3237
反应条件
in tetrahydrofuran 24 h; Heating;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
zinc(II) chloride in acetonitrile 7 h; Heating;
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Kim, Ho-Kyun; Cho, Su-Dong; Kang, Young-Jin; Park, Ki Hun; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthetic Communications, 2005 , vol. 35, # 3 p. 371 - 378
反应条件
1: With hydrazine hydrate in tetrahydrofuran Heating; 2: With PPA in tetrahydrofuran T=130°C; 4 h;
参考文献
Synthesis, , # 4 p. 560 - 564
反应条件
in toluene T=20°C; 0.75 h; Green chemistry;
参考文献
Tetrahedron, , vol. 69, # 17 p. 3530 - 3535
反应条件
1: in toluene RefluxGreen chemistry; 2: With trichlorophosphate in toluene RefluxGreen chemistry; Reagent/catalystTemperatureTimeSolvent;
参考文献
Sung, Gi Hyeon; Lee, In-Hye; Kim, Bo Ram; Shin, Dong-Soo; Kim, Jeum-Jong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Tetrahedron, 2013 , vol. 69, # 17 p. 3530 - 3535