4-氯-苯甲腈N-氧化物合成路线 (共 35 条)
反应条件
in tetrachloromethane
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Synthetic Communications, 1990 , vol. 20, # 9 p. 1373 - 1377
反应条件
in dichloromethane; chloroform 16 h; Heating; Title compound not separated from byproducts;
参考文献
Ennis, Brian C.; Hanhela, Peter J.; Paul, Brenton D.
Australian Journal of Chemistry, 1990 , vol. 43, # 1 p. 109 - 124
反应条件
in acetonitrile T=80°C; 2 h;
参考文献
Jadhav, Ravindra D.; Mistry, Hitesh D.; Motiwala, Hashim; Kadam, Kishorkumar S.; Kandre, Shivaji; Gupte, Amol; Gangopadhyay, Ashok K.; Sharma, Rajiv
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 4 p. 774 - 780
反应条件
1: With triethylamine in chloroform T=20°C; 12 h; 2: With dihydrogen peroxide in chloroform T=20°C; 0.333333 h;
参考文献
Sheng, Shou-Ri; Liu, Xiao-Ling; Xu, Qu; Song, Cai-Sheng
Synthesis, 2003 , # 18 p. 2763 - 2764
反应条件
in dichloromethane T=-20°C; 3 h; Title compound not separated from byproducts;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
in dichloromethane T=-20°C;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
in dichloromethane T=-20°C; 3 h; Title compound not separated from byproducts;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
in diethyl ether
T=0 - 10°C;
参考文献
Baranski, Andrzej
Polish Journal of Chemistry, 1986 , vol. 60, # 4-6 p. 419 - 427
反应条件
1: CHCl3 / 0.75 h / Heating
2: aq. HCl / 0.25 h / Heating
View Scheme
参考文献
Bianchetti,G. et al.
Gazzetta Chimica Italiana, 1963 , vol. 93, p. 1714 - 1725
反应条件
triethylamine in diethyl ether
Ambient temperature;
参考文献
Fisera, Lubor; Jaroskova, Libuse; Matejkova, Iveta; Heimgartner, Heinz
Heterocycles, 1995 , vol. 40, # 1 p. 271 - 278