4-氯-苯甲腈N-氧化物合成路线 (共 35 条)
反应条件
in benzene T=5 - 10°C; 1.5 h;
参考文献
Ogurtsov, V. A.; Rakitin, O. A.; Strelenko, Yu. A.; Obruchnikova, N. V.; Khmel'nitskii, L. I.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 706 - 708
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 742 - 743
反应条件
in diethyl ether Ambient temperature;
参考文献
Rajagopalan,P.
Tetrahedron Letters, 1969 , p. 311 - 312
反应条件
in dichloromethane T=-20°C; 3 h; Title compound not separated from byproducts;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
in dichloromethane T=-20°C; Title compound not separated from byproducts;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
in dichloromethane T=-20°C;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
1: CH2Cl2 / -20 °C 2: CH2Cl2 / Ambient temperature View Scheme
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
in dichloromethane T=-20°C; Title compound not separated from byproducts;
参考文献
Rahmouni, Mustapha; Ko, Yeung Yat Cheng Yeung Lam; Carrie, Robert; Tonnard, Francois
Tetrahedron, 1994 , vol. 50, # 44 p. 12625 - 12632
反应条件
potassium tert-butylate in tetrahydrofuran T=-78°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 19 p. 2703 - 2710
反应条件
in dichloromethane T=0 - 25°C; Molecular sieveInert atmosphere;
参考文献
Xu, Xinfang; Shabashov, Dmitry; Zavalij, Peter Y.; Doyle, Michael P.
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5313 - 5317
反应条件
4-nitro-benzonitrile N-oxide in dichloromethane; chloroform 16 h; Heating;
参考文献
Ennis, Brian C.; Hanhela, Peter J.; Paul, Brenton D.
Australian Journal of Chemistry, 1990 , vol. 43, # 1 p. 109 - 124