4-氯-苯甲腈N-氧化物合成路线 （共 35 条）
反应条件
triethylamine in diethyl ether
参考文献
Alberti, Angelo; Barbaro, Gaetano; Battaglia, Arturo; Guerra, Maurizio; Bernardi, Fernando; et al.
Journal of Organic Chemistry, 1981 , vol. 46, p. 742 - 750
反应条件
1-chlorobenzotriazole in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Umesha; Kumar, K. Ajay; Rai, K. M. Lokanatha
Synthetic Communications, 2002 , vol. 32, # 12 p. 1841 - 1846
反应条件
triethylamine in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Weidner-Wells, Michele A.; Fraga, Stephanie A.; Demers, James P.
Tetrahedron Letters, 1994 , vol. 35, # 35 p. 6473 - 6476
反应条件
triethylamine in diethyl ether T=-5 - 0°C; 0.5 h;
参考文献
Baranski, Andrzej; Shvekhgeimer, Genrikh A.
Polish Journal of Chemistry, 1982 , vol. 56, # 3 p. 459 - 467
反应条件
sodium methylate; acetyl chloride in N,N-dimethyl acetamide T=80 - 85°C;
参考文献
Zen, Shonosuke; Harada, Kazuho
Chemistry Letters, 1982 , p. 1711 - 1714
反应条件
1: hydroxylamine hydrochloride; sodium hydroxide / water; tert-butyl alcohol / 20 °C 2: chloramine-T / water; tert-butyl alcohol / 20 °C View Scheme
参考文献
Rodrigues, Giseli Capaci; Feijo, Daniel Ferreira; Bozza, Marcelo Torres; Pan, Peiwen; Vullo, Daniela; Parkkila, Seppo; Supuran, Claudiu T.; Capasso, Clemente; Aguiar, Alcino Palermo; Vermelho, Alane Beatriz
Journal of Medicinal Chemistry, 2014 , vol. 57, # 2 p. 298 - 308
反应条件
in acetonitrile T=80°C; 2 h;
参考文献
Jadhav, Ravindra D.; Mistry, Hitesh D.; Motiwala, Hashim; Kadam, Kishorkumar S.; Kandre, Shivaji; Gupte, Amol; Gangopadhyay, Ashok K.; Sharma, Rajiv
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 4 p. 774 - 780
反应条件
(i) Et2O, (ii) SOCl2; Multistep reaction;
参考文献
Sen; Seth; Joshi; Rajagopalan
Journal of medicinal chemistry, 1966 , vol. 9, # 3 p. 431 - 433
反应条件
Me3SiN=S=NSiMe3 in benzene T=5 - 10°C; 1.5 h;
参考文献
Ogurtsov, V. A.; Rakitin, O. A.; Strelenko, Yu. A.; Obruchnikova, N. V.; Khmel'nitskii, L. I.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 706 - 708
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 742 - 743
反应条件
1: 34 percent / benzene / 1.5 h / 5 - 10 °C 2: 98 percent / benzene / 48 h / 20 °C View Scheme
参考文献
Ogurtsov, V. A.; Rakitin, O. A.; Strelenko, Yu. A.; Obruchnikova, N. V.; Khmel'nitskii, L. I.
Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 706 - 708
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 742 - 743
