3-正-丁基-2,4-戊烷二酮合成路线 （共 32 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide 6 h; Heating;
参考文献
Mamardashvili, N. Zh.; Semeikin, A. S.; Golubchikov, O. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 6.2 p. 1007 - 1015
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 6 p. 1213 - 1223
反应条件
carbon monoxide; hydrogen; tri-ruthenium(0)dodecacarbonyl in N,N-dimethyl-formamide T=150°C; P=76000.1 Torr; 16 h;
参考文献
Abe, Fujio; Hayashi, Teruyuki; Tanaka, Masato
Chemistry Letters, 1990 , # 5 p. 765 - 768
反应条件
potassium carbonate in acetone Alkylation; 20 h; Heating;
参考文献
Lash, Timothy D.
Tetrahedron, 1998 , vol. 54, # 3-4 p. 359 - 374
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate P=760 Torr; 0.25 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 37, # 17 p. 3009 - 3016
反应条件
boron trifluoride (acetylation);
参考文献
Journal of Organic Chemistry, , vol. 34, # 8 p. 2324 - 2336
反应条件
1: Pd(acac)2/triphenylphosphine / 17 h / 85 - 90 °C 2: H2 / Pd-C / ethyl acetate / 0.25 h / 760 Torr / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 37, # 17 p. 3009 - 3016
反应条件
K5[CoW12O40]*3H2O in neat (no solvent) T=80°C; 0.416667 h;
参考文献
Rafiee, Ezzat; Kahrizi, Masoud; Joshaghani, Mohammad
Chinese Chemical Letters, 2012 , vol. 23, # 12 p. 1363 - 1366
反应条件
boron trifluoride beim Erhitzen des Reaktionsgemisches mit wss. Natriumacetat-Loesung;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3635,3639, 3642
反应条件
boron trifluoride beim Erhitzen des Reaktionsgemisches mit wss. Natriumacetat-Loesung;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3635,3639, 3642
反应条件
dibenzo-18-crown-6; potassium carbonate T=170°C; P=20 Torr; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2159 - 2162
