反应条件
bromobenzene in tetrahydrofuran
(Ar), phenylmagnesiumbromide solution was prepared (ice bath) and was addeed dropwise to Ge-compound, stirred and refluxed for 12 h, added aq. NH4Cl; filtered, removed, diluted with ether, washed with deionized H2O, dried over MgSO4, removed, distilled; elem. anal., NMR, UV, mass. spectra;
参考文献
Bobbitt, Kevin L.; Maloney, Vincent M.; Gaspar, Peter P.
Organometallics, 1991 , vol. 10, p. 2772 - 2777