N,N-二甲基-4-硝基苄胺合成路线 (共 25 条)
反应条件
ammonium hydroxide; iodine T=60°C; 6 h;
参考文献
Iida, Shinpei; Togo, Hideo
Synlett, 2006 , # 16 p. 2633 - 2635
反应条件
1-hydroxy-pyrrolidine-2,5-dione; oxygen; anhydrous cobalt diacetate in acetonitrile T=50°C; 9 h;
参考文献
Cecchetto, Andrea; Minisci, Francesco; Recupero, Francesco; Fontana, Francesca; Franco Pedulli, Gian
Tetrahedron Letters, 2002 , vol. 43, # 19 p. 3605 - 3607
参考文献
Goss; Hanhart; Ingold
Journal of the Chemical Society, 1927 , p. 260
反应条件
palladium 10 on activated carbon; hydrogen in ethanol
参考文献
Murugesan, Dinakaran; Mital, Alka; Kaiser, Marcel; Shackleford, David M.; Morizzi, Julia; Katneni, Kasiram; Campbell, Michael; Hudson, Alan; Charman, Susan A.; Yeates, Clive; Gilbert, Ian H.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 7 p. 2975 - 2990
反应条件
sodium hydroxide in ethanol
参考文献
Toray Industries, Inc.
Patent: US5852030 A1, 1998 ;
US 5852030 A
参考文献
Friedlaender; Mosczyc
Chemische Berichte, 1895 , vol. 28, p. 1141
反应条件
1: 80 percent / acetonitrile 2: 73 percent / aq. sodium hydroxide / 0 °C View Scheme
参考文献
Jemison, Robert W.; Mageswaran, Sivapathasuntharam; Ollis, W. David; Sutherland, Ian O.; Thebtaranonth, Yodhathai
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1154 - 1164
反应条件
HPtCl6·6H2O; 1,1,3,3-tetramethyldisiloxane in tetrahydrofuran; toluene
T=75°C; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040
反应条件
potassium carbonate in water; acetonitrile
T=0 - 50°C; 1 h;
参考文献
F2G LTD
Patent: WO2006/123145 A1, 2006 ;
Location in patent: Page/Page column 58 ;
反应条件
1: With titanium(IV) isopropylate in methanol
T=20°C; Addition;
2: With sodium tetrahydroborate in methanol
T=20°C; Reduction; 1.5 h;
参考文献
Bhattacharyya, Sukanta
Synthetic Communications, 2000 , vol. 30, # 11 p. 2001 - 2008