in neat (no solvent) co-condensation of NMe3 and BCl3 in a glass bulb with slight excess of base at liquid nitrogen temp. in all-glass vacuum system; warming the mixture at ambient temp.; pumping excess of reactants off;;
参考文献
Sreekanth, C. S.; Mok, C. Y.; Huang, H. H.; Tan, K. L.
Journal of Electron Spectroscopy and Related Phenomena, 1992 , vol. 58, p. 129 - 140
