2-苯基-3-(二甲氨基)丙烯醛合成路线 （共 11 条）
参考文献
Pedras, M. Soledade C.; Suchy, Mojmir
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 3 p. 714 - 723
参考文献
Krasnaya, Zh. A.; Stytsenko, T. S.; Bogdanov, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 96 - 100
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 106 - 111
参考文献
Takano, Seiichi; Imamura, Yoko; Ogasawara, Kunio
Heterocycles, 1982 , vol. 19, # 7 p. 1223 - 1225
参考文献
Arnold; Sorm
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 452,455
参考文献
Arnold; Sorm
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 452,455
参考文献
Arnold; Sorm
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 452,455
反应条件
hydrazine hydrate in ethanol Yield given;
参考文献
Takano, Seiichi; Imamura, Yoko; Ogasawara, Kunio
Heterocycles, 1982 , vol. 19, # 7 p. 1223 - 1225
反应条件
1: hydrazine hydrate / ethanol
2: 1.) n-BuLi
3: 1.) t-BuLi / 1.) THF, 0 deg C
4: 1.) BH3Me2S, 2.) H2O2, NaOH
5: pyridine
6: CH3ONa / methanol
View Scheme
参考文献
Takano, Seiichi; Imamura, Yoko; Ogasawara, Kunio
Heterocycles, 1982 , vol. 19, # 7 p. 1223 - 1225
反应条件
(i) brommethylene-dimethyl-ammonium bromide, CHCl3, (ii) H2O; Multistep reaction;
参考文献
Arnold,Z.; Holy,A.
Collection of Czechoslovak Chemical Communications, 1961 , vol. 26, p. 3059 - 3073
反应条件
1: NaOH / ethanol; H2O / 1 h / Heating
2: 310 mg / thionyl chloride / CH2Cl2 / 1 h / 0 °C
3: 54 percent / ammonium thiocyanate / dimethylformamide / 16 h / 70 °C
View Scheme
参考文献
Pedras, M. Soledade C.; Suchy, Mojmir
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 3 p. 714 - 723
